Standard

NEN-EN 14333-3:2004 en

Non fatty foods - Determination of benzimidazole fungicides carbendazim, thiabendazole and benomyl (as carbendazim) - Part 3: HPLC method with liquid/liquid-partition clean up

  • This norm is withdrawn since 28-07-2016

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About norm

Status Withdrawn
Number of pages 13
Committee Voedingsmiddelenanalyse - Horizontale methoden
Published on 01-10-2004
Language English
This document specifies a high performance liquid chromatographic method for the determination of the benzimidazole fungicides carbendazim and thiabendazole in fruits, vegetables and processed products. When benomyl is present, it is completely degraded to carbendazim and is also determined as carbendazim. Thiophanate-methyl is not determined with the method. The method has been validated for carbendazim and thiabendazole in an interlaboratory test with homogenates of apples, French beans, mushrooms, lemons and fruit based infant food. The sample is homogenized with ethyl acetate, sodium hydroxide solution and anhydrous sodium sulfate and the homogenate is filtered. An aliquot portion of the ethyl acetate extract is partitioned with hydrochloric acid solution; the aqueous phase is made alkaline and partitioned with ethyl acetate. The organic layer is evaporated and the residue is dissolved in the HPLC mobile phase. Carbendazim and thiabendazole are determined by reversed-phase high performance liquid chromatography (HPLC) with UV or UV and fluorescence detectors.

Details

ICS-code 67.080.01
Dutch title Vetarme voedingsmiddelen - Bepaling van benzimidazole-fungicides, carbendazim, thiabendazole en benomyl (als carbendazim) - Deel 3: HPLC methode met zuivering door vloeistof/vloeistof partitie
English title Non fatty foods - Determination of benzimidazole fungicides carbendazim, thiabendazole and benomyl (as carbendazim) - Part 3: HPLC method with liquid/liquid-partition clean up
Replaces

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