Standard

NEN-EN 16858:2015 Ontw. en

Foodstuffs - Determination of melamine and cyanuric acid in foodstuffs by liquid chromatography and tandem mass spectrometry (LC-MS/MS)

  • This norm is withdrawn since 30-05-2017

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About norm

Status Withdrawn
Number of pages 22
Committee Voedingsmiddelenanalyse - Horizontale methoden
Published on 01-05-2015
Language English
NEN-EN 16858 specifies a method for the determination of melamine and cyanuric acid in foodstuffs with liquid chromatography in combination with tandem mass spectrometry. The method has been validated in an interlaboratory study via the analysis of spiked samples of milk based infant formula, soy based infant formula, milk powder, whole milk, soy drink and milk chocolate ranging from 0,71 mg/kg to 1,43 mg/kg for melamine and 0,57 mg/kg to 1,45 mg/kg for cyanuric acid. The limits of quantification (LOQ) for melamine and cyanuric acid in food are 0,05 mg/kg and 0,25 mg/kg, respectively. The upper limit of the working range is up to 10 mg/kg for melamine and up to 25 mg/kg for cyanuric acid.

Details

ICS-code 67.050
Dutch title Voedingsmiddelen - Bepaling van melamine en cyanuurzuur in voedingsmiddelen met vloeistofchromatografie en tandem massa spectrometrie (LC-MS/MS)
English title Foodstuffs - Determination of melamine and cyanuric acid in foodstuffs by liquid chromatography and tandem mass spectrometry (LC-MS/MS)
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