Norm

ASTM D7065-11

Standard Test Method for Determination of Nonylphenol, Bisphenol A, p-tert -Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol Diethoxylate in Environmental Waters by Gas Chromatography Mass Spectrometry

61,51

Over deze norm

Status Definitief
Aantal pagina's 13
Commissie D19.06
Gepubliceerd op 15-06-2011
Taal Engels

1.1 This test method covers determination of nonylphenol (NP), nonylphenol ethoxylate (NP1EO), nonylphenol diethoxylate (NP2EO), octylphenol (OP), and bisphenol A (BPA) that are partitioned into organic solvent, separated using gas chromatography and detected with mass selective detection. These compounds or isomer mixtures are qualitatively and quantitatively determined by this method. This method adheres to selected ion monitoring mass spectrometry but full scan mass spectrometry has also been shown to work well under these conditions. Either analysis may be used.

1.2 The method detection limit (MDL) and reporting limit (RL) for NP, NP1EO, NP2EO, OP, and BPA are listed in Table 1.

TABLE 1 MDL and Reporting Limits

Analyte

MDLA, (µg/L)

Reporting RangeB (µg/L)

NP

0.9

5.0-80.0

NP1EO

1.2

10.0-160.0

NP2EO

1.8

20.0-320.0

OP

0.2

1.0-16.0

BPA

0.3

1.0-16.0

A MDL Determined Following The Code of Federal Regulations, 40 CFR Part 136, Appendix B.
B Lowest Point of the Reporting Range is Calculated from the LV1 Concentration Calibration Standard in Table 4.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

Details

ICS-code 71.080.15
Nederlandse titel Standard Test Method for Determination of Nonylphenol, Bisphenol A, p-tert -Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol Diethoxylate in Environmental Waters by Gas Chromatography Mass Spectrometry
Engelse titel Standard Test Method for Determination of Nonylphenol, Bisphenol A, p-tert -Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol Diethoxylate in Environmental Waters by Gas Chromatography Mass Spectrometry

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