Norm

ASTM D7644 - 10e2 en

Standard Test Method for Determination of Bromadiolone, Brodifacoum, Diphacinone and Warfarin in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)

  • Deze norm is ingetrokken sinds 01-02-2016

57,20 69,21 Incl BTW

Over deze norm

Status Ingetrokken
Aantal pagina's 15
Gepubliceerd op 01-06-2010
Taal Engels

1.1 This procedure covers the determination of bromadiolone, brodifacoum, diphacinone and warfarin (referred to collectively as rodenticides in this test method) in water by direct injection using liquid chromatography (LC) and detected with tandem mass spectrometry (MS/MS). These analytes are qualitatively and quantitatively determined by this method. This method adheres to multiple reaction monitoring (MRM) mass spectrometry.

1.3 UnitsThe values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

TABLE 1 Detection Verification Level and Reporting Range

AnalyteDVL
(ng/L)
Reporting Range
(ng/L)
Bromadiolone20125-2500
Brodifacoum20125-2500
Diphacinone20125-2500
Warfarin20125-2500


FIG. 1 Example Primary SRM Chromatograms Signal/Noise Ratios


FIG. 2 Example Confirmatory SRM Chromatograms Signal/Noise Ratios

Details

ICS-code 13.060.50
Engelse titel Standard Test Method for Determination of Bromadiolone, Brodifacoum, Diphacinone and Warfarin in Water by Liquid Chromatography/Tandem Mass Spectrometry (LC/MS/MS)
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