Norm

ISO 20899:2018 en

Water - Plutonium en neptunium - Beproevingsmethode met ICP-MS

73,95 89,48 Incl BTW

Over deze norm

Status Definitief
Aantal pagina's 13
Commissie Radioactiviteit - Toepassing en meten
Gepubliceerd op 01-09-2018
Taal Engels
ISO 20899 specifies methods used to determine the concentration of plutonium and neptunium isotopes in water by inductively coupled plasma mass spectrometry (ICP-MS) (239Pu, 240Pu, 241Pu and 237Np). The concentrations obtained can be converted into activity concentrations of the different isotopes[9]. Due to its relatively short half-life and 238U isobaric interference, 238Pu can hardly be measured by this method. To quantify this isotope, other techniques can be used (ICP-MS with collision-reaction cell, ICP-MS/MS with collision-reaction cell or chemical separation). Alpha spectrometry measurement, as described in ISO 13167[10], is currently used[11]. This method is applicable to all types of water having a saline load less than 1 g·l−1. A dilution of the sample is possible to obtain a solution having a saline load and activity concentrations compatible with the preparation and the measurement assembly. A filtration at 0,45 μm is needed for determination of dissolved nuclides. Acidification and chemical separation of the sample are always needed. The limit of quantification depends on the chemical separation and the performance of the measurement device.

Details

ICS-code 13.060.60
13.280
17.240
Nederlandse titel Water - Plutonium en neptunium - Beproevingsmethode met ICP-MS
Engelse titel Water quality - Plutonium and neptunium - Test method using ICP-MS

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