Norm

NEN-EN 14526:2015 Ontw. en

Voedingsmiddelen - Bepaling van saxitoxine en decarbamoyl saxitoxine in schaaldieren - HPLC methode bij gebruik van voorloopkolomderivatie met peroxide of periodaat oxidatie

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Status Ontwerp
Aantal pagina's 67
Commissie Voedingsmiddelenanalyse - Horizontale methoden
Gepubliceerd op 01-04-2015
Taal Engels
This document specifies a method for the quantitative determination of saxitoxin (STX), decarbamoyl saxitoxin (dcSTX), neosaxitoxin (NEO), decarbamoyl neosaxitoxin (dcNEO), gonyautoxin 1 and 4 (GTX1,4; sum of isomers), gonyautoxin 2 and 3 (GTX2,3; sum of isomers), gonyautoxin 5 (GTX5 also called B1), gonyautoxin 6 (GTX6 also called B2), decarbamoyl gonyautoxin 2 and 3 (dcGTX2,3; sum of isomers), N-sulfocarbamoyl-gonyautoxin 1 and 2 (C1,2; sum of isomers) and (depending on the availability of certified reference materials (CRMs)) N-sulfocarbamoyl-gonyautoxin 3 and 4 (C3,4; sum of isomers) in (raw) mussels, oysters, scallops and clams. Laboratory experience has shown, that it is also be applicable in other shellfish, and cooked shellfish products. The method described was validated in a collaborative study, and published as AOAC Official Method. This method was also verified in a EURL-performance test aiming the total toxicity of the samples. Toxins which were not available in the first collaborative study, as dcGTX2,3 and dcNEO were validated in two additional studies. The lowest validated levels, are given in μg toxin (free base) per kg shellfish meat and also as μmol/kg shellfish meat and are listed in Table 1.

Details

ICS-code 67.120.30
Nederlandse titel Voedingsmiddelen - Bepaling van saxitoxine en decarbamoyl saxitoxine in schaaldieren - HPLC methode bij gebruik van voorloopkolomderivatie met peroxide of periodaat oxidatie
Engelse titel Foodstuffs - Determination of saxitoxin-group toxins in shellfish - HPLC method using pre-column derivatization with peroxide or periodate oxidation
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