Norm

NEN-EN 16215:2011 Ontw. en

Diervoeder - Bepaling van dioxinen en dioxine-achtige Polychloorbifenylen (PCB's) en indicator Polychloorbifenylen (PCB's) met behulp van Gas Chromatografie / Hoge Resolutie Massa Spectrometrie (GC/HRMS)

  • Deze norm is ingetrokken sinds 02-05-2012

35,70

Over deze norm

Status Ingetrokken
Aantal pagina's 50
Commissie Diervoeder
Gepubliceerd op 01-01-2011
Taal Engels
This European Standard describes a procedure for the determination of polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs), (together termed 'dioxins') and dioxin-like and non dioxinlike PCBs (dl-PCBs and ndl-PCBs) in animal feeding stuffs. Collaborative studies have been carried out. The method is suitable for the determination of dioxins, dl-PCBs and ndl-PCBs at the appropriate MRL in compound feed and ingredients e.g. oil, mineral clay. The method is applicable to samples containing residues of one or more of the following dioxins, dioxin-like PCBs and indicator PCBs. The limit of quantification (LOQ) for the relevant individual congeners of dioxins/furans is 0,05 pg/g (OCDD/F = 0,1 pg/g), of non-ortho PCBs 0,05 pg/g, of mono-ortho PCBs 10 pg/g and of indicator PCBs 100 pg/g. For determination of dioxins and dioxin-like PCBs, the procedure can be used as confirmatory method as defined by Regulation (EC) No 152/2009 for dioxins and dl-PCB in feed. Confirmatory methods are highresolution gas chromatography/high resolution mass spectrometry (HRGC/HRMS) methods. If only the analysis of indicator PCBs is required, a GC-LRMS method can be used (e.g EN 15741 Animal feeding stuffs - Determination of OCpesticides and PCBs by GC/MS [7] and EN 15742 Animal feeding stuffs - Determination of OCpesticides and PCBs by GC/ECD) provided that appropriate analytical performance criteria are met in the relevant range for the matrix of interest.

Details

ICS-code 65.120
Nederlandse titel Diervoeder - Bepaling van dioxinen en dioxine-achtige Polychloorbifenylen (PCB's) en indicator Polychloorbifenylen (PCB's) met behulp van Gas Chromatografie / Hoge Resolutie Massa Spectrometrie (GC/HRMS)
Engelse titel Animal feed - Determination of dioxins and dioxin-like PCBs by GC/HRMS and of indicator PCBs by GC/HRMS
Vervangen door
Normatieve verwijzingen
  • 70/373/EG, Analysemethoden

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