Norm

NEN-EN 17053:2018 en

Diervoeder: Methoden van bemonstering en analyse - Bepaling van sporenelementen, zware metalen en andere elementen in diervoeders door ICP-MS (multi-methode)

62,22 75,29 Incl BTW

Over deze norm

Status Definitief
Aantal pagina's 29
Commissie Diervoeder
Gepubliceerd op 01-01-2018
Taal Engels
NEN-EN 17053 specifies a method for the determination of trace elements, heavy metals and other elements in animal feed by inductively coupled plasma mass spectrometry (ICP-MS). The method is used to determine As, Cd, Co, Cu, Fe, Hg, Mn, Mo, Pb, Se, Tl, U and Zn in the extraction solution after pressurized digestion. For the determination of extractable lead in minerals and feeds containing phyllosilicates (e.g. kaolinite clay) wet digestion with nitric acid should be used. The method described is suitable for use in quadrupole instruments equipped either with or without additional technology to reduce molecular ion interferences (e.g. collision or reaction technologies) as well as in high-resolution sector-field systems. The method was fully statistically tested and evaluated in a collaborative trial comprising eight animal feeding stuff samples for the elements As, Cd, Co, Cu, Fe, Hg, Mn, Mo, Pb, Se, Tl, U and Zn. For elements with a HORRAT value higher than 2 (e.g. mercury, see Annex A) the method is more applicable as a screening method and not for confirmatory purposes. High-resolution sector-field ICP-MS was not tested in the validation ring trial. The limit of quantification for each element is dependent on the sample matrix as well as the instrument. For the elements Co, Mn, Mo, Pb, Tl, U a limit of quantification of 0,10 mg/kg should normally be obtained, for the elements Fe and Zn 5,0 mg/kg, while for Cd 0,03 mg/kg, Hg 0,04 mg/kg and As 0,05 mg/kg should normally be quantifiable. Details on the successfully tested working range for each element are described in this standard.

Details

ICS-code 65.120
Nederlandse titel Diervoeder: Methoden van bemonstering en analyse - Bepaling van sporenelementen, zware metalen en andere elementen in diervoeders door ICP-MS (multi-methode)
Engelse titel Animal feeding stuffs: Methods of sampling and analysis - Determination of trace elements, heavy metals and other elements in feed by ICP-MS (multi-method)
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